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To the twelve-minute attempt (Fig. 3F), the enormous diamond grains will be the head composition, while the evidenced by the inset FFT image of diamond (111) diffraction places and the Raman range in the Si Appendix, Fig. S5, that is like the brand new 0-min try, confirming the graphite provides completely changed into diamond and shaped a mass diamond amazingly weighed against the initial (two to four min) and you will next schedules (6 to 8 min). This type of efficiency certainly check if the new mixed appearance of diamond (111) and you may graphite (002) regarding the try 8-minute is actually a great transitional several months away from graphite to diamond. Fake diamond plays a crucial role from the production community, jewellery, and you may upcoming photoelectronic devices, however it is a button issue to prepare the desired higher-area expensive diamonds.
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At the same time, a good flake-for example diamond amazingly (reddish image within the Fig. 2D-2) signifies that diamond begins to arrive, within the a great agreement for the SEM and you will Raman spectra. To your 120-s sample, of a lot nanodiamond crystals naked on the side of cauliflower-including dirt safeguarded the newest graphite nanorods (Fig. 2E-2). These overall performance prove the brand new NCD characteristics present in the new Raman spectrum.